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Print: ISSN 0914-4935
Online: ISSN 2435-0869
Sensors and Materials
is an international peer-reviewed open access journal to provide a forum for researchers working in multidisciplinary fields of sensing technology.
Online: ISSN 2435-0869
Sensors and Materials
is an international peer-reviewed open access journal to provide a forum for researchers working in multidisciplinary fields of sensing technology.
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Sensors and Materials
is covered by Science Citation Index Expanded (Clarivate Analytics), Scopus (Elsevier), and other databases.
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Sensors and Materials
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is covered by Science Citation Index Expanded (Clarivate Analytics), Scopus (Elsevier), and other databases.
Instructions to authors
English 日本語
Instructions for manuscript preparation
English 日本語
Template
English
Publisher
MYU K.K.
Sensors and Materials
1-23-3-303 Sendagi,
Bunkyo-ku, Tokyo 113-0022, Japan
Tel: 81-3-3827-8549
Fax: 81-3-3827-8547
MYU Research, a scientific publisher, seeks a native English-speaking proofreader with a scientific background. B.Sc. or higher degree is desirable. In-office position; work hours negotiable. Call 03-3827-8549 for further information.
MYU Research
(proofreading and recording)
MYU K.K.
(translation service)
The Art of Writing Scientific Papers
(How to write scientific papers)
(Japanese Only)
Sensors and Materials, Volume 32, Number 4(3) (2020)
Copyright(C) MYU K.K.
Copyright(C) MYU K.K.
|
pp. 1511-1522
S&M2198 Research Paper https://doi.org/10.18494/SAM.2020.2649 Published: April 30, 2020 Transformation from anatase to rutile titania using hydrothermal method: Investigation of morphology and thermal stability [PDF] Mpanza P. Ntsikelelo, Malevu D. Thembinkosi, Lehloonolo F. Koao, Motloung V. Setumo, and Motaung E. Tshwafo (Received October 4, 2019; Accepted February 2, 2020) Keywords: titanium dioxide, nanocrystal, annealing temperature, phase transformation
Titanium dioxide nanoparticles were successfully synthesized using the hydrothermal
method in an autoclave at 100 °C. The onset of the formation of the rutile phase from 400 to
700 °C was investigated through the morphology, structure and thermal properties. X-ray
diffractometer and Raman spectroscopy confirmed the formation of a hybrid anatase (A) and
rutile (B) phase at 400 °C. The nanoparticles formed spherical structures with an average size
between 19.799 and 38.685 nm. Thermogravimetric analysis confirmed that a TiO2 nanocrystal
subjected to higher temperatures undergoes four degradation stages involving the desorption
of water molecules, the loss of organic compounds, and the phase change from amorphous to
crystalline anatase.
Corresponding author: Motaung E. Tshwafo  This work is licensed under a Creative Commons Attribution 4.0 International License. Cite this article Mpanza P. Ntsikelelo, Malevu D. Thembinkosi, Lehloonolo F. Koao, Motloung V. Setumo, and Motaung E. Tshwafo, Transformation from anatase to rutile titania using hydrothermal method: Investigation of morphology and thermal stability, Sens. Mater., Vol. 32, No. 4, 2020, p. 1511-1522. |
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